It gives me immense pleasure in presenting this book to students who have opted for Chemistry as a major subject at their graduation level. This book will definitely help students in their preparation of Analytical chemistry paper-IV. Multiple choice questions are useful in thorough study of any subject. This book comprises of 240 MCQ's from all the topics of semester five and six. I am grateful to my daughter Sonia for her sincere support and unlimited cooperation in shaping this book. My heartfelt thank you to my husband and parents, without their backing its just not possible.